CHM 2046L 24-Lab (2856) General Chemistry Laboratory II
Summer 2018
Meeting
Information: Face
to Face
Course Location: TS-DE433
Meeting Days: Tuesday
and Thursday
Class
Times: 2:00 – 4:00 PM
Instructor: Chris
Lue, Ph.D.
Cell
# 404-668-1757
Contact: lue.chris@spcollege.edu
Office Hours:
Mon.
and Wed. 5:00 – 6:00 PM
Tues
and Thurs. 10:00 – 11:00 AM and 1:00 – 1:45 PM
Office
hours are held in the Learning Support Center TS-FA 154
Course
Info: This
course is a continuation of General Chemistry Laboratory I. It includes some Qualitative Analysis.
Corequisite: CHM
2046
Text: Custom CHEM Lab Manual 2046L (Cengage)
ISBN:
9781337041577
Required: •
Safety goggles (NOT glasses), approved for use in chemical laboratories (American
National Standards Institute (ANSI) Z-87.1-1989)
•
Lab coat (required if not wearing long pants)
•
Latex/nitrile gloves (optional)
•
One laboratory notebook (glued or sewn binding)
•
A non-programmable scientific calculator (TI-30x II, or similar)
Criteria
Performance Standard:
Upon the completion of this course the
student will, with a minimum 70 percent accuracy, demonstrate mastery of each
of the stated objectives through classroom measures developed by individual
course instructors.
Student/Classroom
Expectations:
Students are expected to read the
related sections of the lab manual and complete the prelab prior to coming to class. Students are expected to complete lab
reports according to the policies outlined in this syllabus. It is the student’s
responsibility to obtain missed work when absent from class.
Academic
Department:
Dean: Nativea Middleton
Office Location: UP 337B (Seminole Campus)
Office Number: 727-394-6995
Academic Chair: Mike
Davis
Office Location: LY 206
Office Number: 727-712-5245
FREE
TUTORS: In the LSC, CL LA-100 and TS FA154
COLLEGE
CALENDAR: https://go.spcollege.edu/calendar/.
Important Dates:
May 14 Classes begin
May 18 Last day to
withdraw with refund
May 28 Memorial Day –
COLLEGE CLOSED
June 14 Last day to withdraw with a grade of “W”
July 4 Independence
Day – COLLEGE CLOSED
July 17-18 Final Exams
Attendance
Out of respect for the instructor and
fellow students, please be on time to class. If you miss the prelab lecture,
you will be asked to leave the lab. Attendance will be verbally recorded for
the first two weeks of the semester. If you are not attending this class during
this time, you will be automatically dropped from the course, per SPC
regulations. For the benefit of other students, please refrain from coming to
class ill. Missed labs cannot be made up, but the lowest grade for one
laboratory report will be dropped.
At the 60% mark of the semester, if you have missed or have failed to
submit reports from three or more lab meetings, you will fail to meet my
criteria for active participation and will be withdrawn and given a “WF” for
the course. After the 60% mark you will receive an “F” for the course. The college-wide attendance policy is
included in the “Addendum to the Syllabus”, which should be read at the
following web address: http://www.spcollege.edu/addendum/.
Faculty must
file lack of attendance reports (exceeding 2 absences) for veterans,
dual-enrolled, Early College and Collegiate High School students.
Faculty members are unable to withdraw a
student from their course. If a student wishes to withdraw from this class
before the final date set for withdrawals, this student must initiate a W
online. Failure to withdraw from a class before the set date, June 14, 2018, will result in an “F” or “WF” for the
course. If a student withdraws from the lecture class, the student must also
withdraw from the co-requisite 2046 lab. Please see me before withdrawing from
the class.
Course
Goals and Objectives
CHM 2046L includes
dealing with kinetics,
acid-base and solubility equilibria, selected reactions of metals and nonmetals,
and qualitative elemental analysis laboratory experiments,
which are quantitative in nature and designed to give practice in acceptable
laboratory techniques. The class is designed for students who
have a good understanding of the concepts presented in CHM 2045L. The sequence of CHM 2045L and CHM 2046L is
designed to meet first-year college chemistry requirements for science majors
and engineering students.
Safety
1.
Lab
Dress Code:
• Shoes, not sandals or open shoes, are required in the lab
at all times.
• Due to the probable spillage of water and the floor
becoming slippery, rubber
soled shoes, such as tennis shoes, are best.
• Shorts or skirts will not be worn. They will not keep
solutions from splattering
on your legs. Blue jeans may be the best type of lab wear.
• Belly-button policy: Shirts that expose your
midriff are not permitted in lab. The
bench
top is near your waist level, so spills there will be common. A buttoned lab coat
covering the midriff is acceptable.
• Safety goggles are required at all times in the lab.
• If you are wearing contact lenses in the lab, you must
notify the instructor in case of an accident.
• Prescription glasses are acceptable with safety goggles.
Penalties:
• First violation - you will be sent to
change your clothes to come under compliance.
•
Second violation – you will receive a zero for that lab.
• Safety glasses – students not wearing
safety glasses while inside the laboratory will be asked to leave the lab and
will receive a zero for the current
experiment.
2.
Broken
glass must be disposed of in the appropriate container; notify instructor in
the event of broken glassware.
Before Laboratory Class
1. The experiment must be read prior to
coming to lab. Pay particular attention to the safety precautions.
2. Write a detailed procedure for the
experiment in your laboratory notebook.
The procedure should be detailed enough so that you can perform the
experiment without consulting the lab manual.
3. Complete the Advance Study Assignment
(ASA) in the laboratory manual.
4.
There is an online pre-lab reading quiz
to make sure you have an understanding of the general lab concepts before coming
to lab. The quiz will close 3 hrs. before lab. Each quiz is worth 10 points.
5. The previous week’s lab experiment
report (including ASA) must be turned in at the beginning of the lab period. Late
lab reports will be accepted up to 1 week late with a 10
point penalty.
During Laboratory Class
You
must strictly adhere to the dress code.
Electronic Communications Devices: Cell phones must be turned off or in vibrate mode and
put away during lab.
1. Have the procedure and ASA acknowledged
with a stamp before beginning the lab.
2. A short lab lecture will be given to
explain various experimental considerations. It is your responsibility to ask
questions about any procedures that you do not understand.
3. Safety goggles must be worn at all times
while in the laboratory. Even if you are finished the lab, other students may
still be working with dangerous chemicals. Prescriptions glasses or sunglasses
are not considered safety goggles.
4.
All
data are collected in your laboratory notebook. You must record experimental
data directly in your laboratory notebook as well as on the report sheet from
the laboratory manual. All data must
be recorded using pens and NOT pencils. If a correction needs to be
made, simply draw a single line through it and write the corrected information
above or below it. Under no circumstances, should white out be used.
5.
Most
experiments will be worked with a partner.
Please work with the person sitting NEXT to you. No more than two people are to work
together at one time unless I approve it.
All calculations, conclusions, and other report answers are to be done
independently of your partner or anyone else.
Students MAY NOT SHARE answers,
conclusions, or results. Sharing and copying work is considered cheating.
(See SPC Student Handbook for information on this subject.)
6. After completing your experiment, your
equipment should be cleaned and returned. Your lab bench must be clean.
7. Before leaving the lab, you should
have your data and notebook acknowledged with a stamp. When you turn
in your lab report, it will be stamped with the received date. Lab
reports that do not have both the acknowledgement and received stamps will not
be given credit.
Grading
Each laboratory report (including the
ASA) is worth 100 points (800 points total after the lowest report dropped).
The prelab quizzes are worth 10 points each (80 points total after the lowest
one dropped). The safety quiz is worth
100 points. Each entry in the lab notebook counts as 10 points (80 points total
with one dropped). There is a final lab quiz, which is worth 100 points.
The following is the point distribution for this course:
Category |
Points |
Safety
Quiz |
100 |
Prelabs |
80 |
Lab
Reports |
800 |
Laboratory
Notebook |
80 |
Final
Quiz |
100 |
Your laboratory reports, quizzes, and notebook
will be totaled to determine your final grade using the following scale:
1,044
– 1,160 points (90% and above) A
928 – 1,043 points (80%-89%) B
812 – 927 points (70%-79%) C
696 – 813 points (60%-69%) D
<696 points (Below 60%) F
Academic
Honesty
If you are caught cheating on a
laboratory report or the practical, I will recommend you receive a “WF” for the
course. Cheating and plagiarizing does not benefit you or your classmates.
Please refer to your Supplement to the Faculty, Staff and Student Handbook,
page 15 (or online at http://www.spcollege.edu/academichonesty/) for a definition of cheating and plagiarism. There is no
tolerance for cheating and academic dishonesty.
No
cell phones, iPods, or other electronic devices except a NON-GRAPHING
calculator may be used for the practical. Students caught looking at or using
such devices during the practical will be considered cheating. Also, taking
pictures of or copying questions from any exam will also be consider cheating.
Exam and quiz questions along with periodic tables must be turned in with
answer sheets.
Class
Participation and Etiquette
Please
turn off cellular telephones, iPods and other electronic devices prior to
entering class! All
notes should be taken in you laboratory notebook. Please stay on task. If you cannot stay on
task, I reserve the right to excuse you from the laboratory.
Special Accommodations
If you wish to
receive special accommodations as a student with a documented disability,
please make an appointment with Elizabeth
Shumate
at 727-712-5789. If you have a documented hearing loss, please contact the
Program for the Deaf at 727-791-2628 (V/TDD). If you will need assistance
during an emergency classroom evacuation, it is imperative that you speak with Elizabeth Shumate immediately
about arrangements for your safety.
Campus
Safety and Security
For
information about campus safety and security policies please contact
727-791-2560. For information about sexual offenders on your campus please
contact campus security or the associate provost office, or for general
information go to the State of Florida website at http://www3.fdle.state.fl.us/sopu/index.asp.
Pay attention to the experiment
numbers, which are not in the same order as the manual.
Laboratory Meeting |
Laboratory Dates |
Experiment Number |
Experiment
Description |
1 |
5/15 *Add/Drop Week |
– |
Check-in and safety
rules |
|
5/17 |
– |
no lab |
2 |
5/22 |
handout |
Safety Quiz Freezing Point
Depression |
3 |
5/24 |
2 |
Rates of Chemical
Reactions. The Iodination of Acetone |
– |
5/29 |
– |
Study Hall |
4 |
5/31 |
2 |
Rates of Chemical
Reactions. The Iodination of Acetone |
5 |
6/5 |
3 |
Determination of an Equilibrium Constant for a Chemical
Reaction |
6 |
6/7 |
4 |
Properties of Systems in Chemical Equilibrium–Le Chatelier's Principle |
7 |
6/12 |
5 |
Determination of the Hardness of Water |
8 |
6/14 *Last Day to Withdraw |
6 |
pH Measurements-Buffers and Their Properties |
9 |
6/19 |
6 |
pH Measurements-Buffers and Their Properties |
10 |
6/21 |
7 |
Qualitative Analysis of Group I Cations |
– |
6/26 |
– |
Study Hall |
11 |
6/28 |
9 |
The Ten Test Tube Mystery |
12 |
7/3 |
9 |
The Ten Test Tube Mystery |
13 |
7/5 |
10 |
Determination of Iron by Reaction with Permanganate-A
Redox Titration |
14 |
7/10 |
11 |
Determination of an Equivalent Mass by Electrolysis |
15 |
7/12 |
– |
Final Quiz |
– |
7/17 |
– |
Study Hall |
Resources: I will be available during office hours to
answer any questions you have. Also,
there are (FREE) tutors in FA 154, who can help you at times when Imay not be available.
For non-academic resources, please see: http://www.spcollege.edu/appeals.
After reading
this syllabus, read this signature page, sign it and hand it to your
instructor.
Signature Page
I have read,
understand, and agree to abide fully by the parameters set in this syllabus and
Syllabus Addendum.
Student
Signature: Date: .